Journal
INORGANIC CHEMISTRY
Volume 40, Issue 20, Pages 5292-+Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ic010060l
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The complex bis-5,5 '-(1,3-propanediyldiimino)-2,2-dimethyl-4-hexen-3-onato samarium bis(trimethylsilyl)amido is a solvent- and halide-free anhydrous, monomeric lanthanide Schiff base complex. It was synthesized from triflate-derived homoleptic Sm[N(TMS)(2)](3) and isolated in excellent yields and analytical purity. For larger rare earths, only dimers were observed using analogous reaction pathways.
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