Journal
TETRAHEDRON
Volume 57, Issue 41, Pages 8647-8651Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4020(01)00859-6
Keywords
rhazinilam; alkylation; thiophenylimine; pyrrole
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2-Piperidone has been converted into (+/-)-rhazinilam in nine steps in 8% overall yield. The key transformation involves the conversion of the lactam 5 into the annulated pyrrole derivative 3 via the thiophenyl imine 8. (C) 2001 Published by Elsevier Science Ltd.
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