Journal
INORGANIC CHEMISTRY
Volume 40, Issue 22, Pages 5719-+Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ic0103852
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A convenient solvothermal synthesis of SnS nanoparticles from activated tin metal and elemental sulfur is reported. Through the use of diethyleneglycoldimethylether (diglyme) as a solvent, unprotected particles of Herzenbergite 20-40 nm in size were obtained at a reaction temperature of 160 degreesC. Powder X-ray diffraction (XRD), EDX analysis, and TEM studies showed that beta -SnS is the only product.
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