Journal
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
Volume 20, Issue 11, Pages 649-661Publisher
ELSEVIER SCI LTD
DOI: 10.1016/S0165-9936(01)00121-2
Keywords
pesticides; matrix modification; extraction; clean-up; determination
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The importance of matrix pretreatment, sample extraction and clean-up in multiresidue methods for pesticide analyses is discussed, with emphasis on alternative new techniques attempted worldwide such as accelerated solvent extraction, microwave-assisted extraction, solid-phase extraction, solid-phase micro-extraction, matrix solid-phase dispersion, supercritical fluid chromatography, ultrasonic extraction and gel permeation chromatography. Detection employing capillary gas chromatography and high-performance liquid chromatography in conjunction with mass spectrometry, capillary electrophoresis, immunoassay techniques and others is summarized. (C) 2001 Elsevier Science B.V. All rights reserved.
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