Journal
ORGANIC LETTERS
Volume 3, Issue 22, Pages 3553-3555Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol016668f
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- NIGMS NIH HHS [GM28553] Funding Source: Medline
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[GRAPHICS] Retrocycloadditions of 4H-4-alkyl-5-(trialylsilyloxy)-1,3-dioxins proceed smoothly in refluxing toluene to afford (Z)-2-(trialkylsilyloxy)-2-alkenals with complete stereos electivity. These enals undergo Sasaki-type [4 + 3] cyclizations with dienes in the presence of Lewis acids, in many instances with excellent regio- and/or stereoselectivity.
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