Journal
MATERIALS RESEARCH BULLETIN
Volume 36, Issue 13-14, Pages 2339-2346Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0025-5408(01)00734-6
Keywords
semiconductors; nanostructures; chemical synthesis; X-ray diffraction
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Bi2S3 nanorods, with a diameter of ca. 10 nm and a length of up to ca. 300 nm, have been successfully prepared from a formaldehyde solution of bismuth nitrate and thiourea by microwave irradiation. Powder X-ray diffraction (XRD) pattern indicates that the product is pure orthorhombic Bi2S3 phase. The product is also characterized by the techniques of transmission electron microscopy (TEM) and X-ray photoelectron spectra (XPS). (C) 2001 Elsevier Science Ltd. All rights reserved.
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