Journal
CARBOHYDRATE RESEARCH
Volume 336, Issue 1, Pages 75-78Publisher
ELSEVIER SCI LTD
DOI: 10.1016/S0008-6215(01)00231-2
Keywords
primary alcohol oxidation; glucaric acid; nitroxide; bleach
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The oxidation of D-( +)-glucose to D-glucaric acid using the TEMPO-like nitroxide oxidation catalyst, 4-acetamido-2,2,6,6-tetramethyl-l-piperidinyloxy (4-acetamido-TEMPO) was carried out using several oxidizing agents and co-catalyst. The pH and temperature of the reactions were closely monitored to decrease degradations during the oxidation, and several isolation methods were explored. (C) 2001 Elsevier Science Ltd. All rights reserved.
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