Journal
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS
Volume 57, Issue -, Pages M506-M508Publisher
INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S1600536801016208
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The title complex, bis(acetylacetonato)diaquanickel(II) monohydrate, [Ni(C5H7O2)(2)(H2O)2)].H2O, was easily synthesized in high yield by electrochemical dissolution of nickel metal in an acetylacetone and ethanol solution via direct hydrolysis of the electrolyte solution at a temperature of 333 K. The crystal structure shows octahedral coordination of nickel with two trans aqua ligands. An uncoordinated water molecule engages in hydrogen bonding.
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