Journal
TETRAHEDRON LETTERS
Volume 42, Issue 46, Pages 8211-8213Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(01)01627-6
Keywords
1-aminoalkyl phosphonates; aldehydes; alumina; microwave; amines
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A simple, efficient and general method has been developed for the synthesis of 1-aminoalkyl phosphonates through a one-pot reaction of aldehydes with amines in the presence of acidic alumina under solvent-free conditions using microwave irradiation. It was also found that acidic alumina supported ammonium formate under solvent-free conditions is capable of the synthesis of I-aminophosphonates from aldehydes and diethyl phosphite under mild reaction conditions. (C) 2001 Published by Elsevier Science Ltd.
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