Journal
JOURNAL OF ALLOYS AND COMPOUNDS
Volume 329, Issue 1-2, Pages 168-172Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/S0925-8388(01)01581-X
Keywords
rare earth compounds; crystal growth; crystal structure; X-ray diffraction; TEM
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New rare-earth boron-rich solids of the composition REB28.5C4 (Re = Y, Ho, Er, Tm and Lu) were synthesized by solid state reaction and single crystals were grown using a high temperature metal solution method. The structure was solved by a direct method from single crystal X-ray diffraction data with Y-B-C as a representative. It shows a layered structure with trigonal symmetry (space group: R (3) over barm (No. 166)) and the unit cell parameters are: a = b = 5.6457(9) Angstrom, c = 56.8873(13) Angstrom. (C) 2001 Elsevier Science B.V. All tights reserved.
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