Journal
TETRAHEDRON LETTERS
Volume 42, Issue 48, Pages 8489-8491Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(01)01817-2
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We have demonstrated the syntheses of enantiomerically enriched tricyclo[4.2.1.0(3.8)]nonanes from C-s symmetric cyclohexanones by means of enantio selective deprotonation, followed by an intramolecular Michael-aldol reaction. The asymmetric deprotonation was achieved in up to 79% ee and the following Michael-aldol reaction gave the corresponding tricyclononanes with almost the same optical purity. (C) 2001 Elsevier Science Ltd. All rights reserved.
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