Journal
ORGANIC LETTERS
Volume 3, Issue 26, Pages 4173-4176Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol016792z
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- NHLBI NIH HHS [HL-58114] Funding Source: Medline
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[GRAPHICS] A new tin recycling method for Stille couplings catalytic in tin is reported. PMHS made hypercoordinate by KF(aq) allows Me3SnH to be efficiently recycled during a Pd(0)-catalyzed hydrostannation/Stille cascade. Relative to previously disclosed protocols, reaction times are shorter and because this process is believed to proceed through a Me3SnF intermediate the hazards and problems associated with trimethyltins are also diminished.
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