Journal
TETRAHEDRON LETTERS
Volume 43, Issue 3, Pages 523-525Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(01)02184-0
Keywords
marine metabolites; steroid glycosides; two-dimensional NMR spectroscope
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The structure of mycaloside A (1) isolated front the Caribbean sponge Mycale laxissima has been established as (22E,20R,24S)-3-O-{alpha-D-Gelp(1-->2)-beta-D-Arap(1-->3)-[beta-D-Gelp(1-->4)]-beta-D-Glep}-3beta,4beta,15alpha,21-tetrahydroxy-24-methylcholesta-5,22-diene by interpretation of spectral data and chemical transformations. (C) 2002 Elsevier Science Ltd. All rights reserved.
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