Journal
MICROSCOPY AND MICROANALYSIS
Volume 8, Issue 1, Pages 21-28Publisher
CAMBRIDGE UNIV PRESS
DOI: 10.1017/S143192760201005X
Keywords
wet-ETEM; in situ liquid-solid reactions on the nanoscale; liquid hydrogenation and polymerization
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We present the development of in situ wet environmental transmission electron microscopy (Wet-ETEM) for direct probing of controlled liquid-catalyst reactions at operating temperatures on the nanoscale. The first nanoscale imaging and electron diffraction of dynamic liquid hydrogenation and polymerization reactions in the manufacture of polyamides reported here opens up new opportunities for high resolution studies of a wide range of solution-solid and solution-gas-solid reactions in the chemical and biological sciences.
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