Journal
ANALYTICAL AND BIOANALYTICAL CHEMISTRY
Volume 372, Issue 4, Pages 562-568Publisher
SPRINGER HEIDELBERG
DOI: 10.1007/s00216-001-1120-y
Keywords
soxhlet extraction; ASE; microwave-assisted extraction; ultrasonic extraction; fluidized-bed extraction; chlorinated compounds
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The performance of various enhanced extraction techniques, such as accelerated solvent extraction, microwave-assisted extraction, Soxhlet extraction, ultrasonic extraction and fluidized-bed extraction for the determination of polychlorinated organic compounds in dry sediment was investigated in two laboratories. The results of the two laboratories were in good agreement. The extraction yields from the batch extraction methods were lower than those from the dynamic techniques. Accelerated solvent extraction, especially, exhibited higher extraction efficiency than the standard procedure, Soxhlet extraction, whereas the results of fluidized-bed extraction were comparable.
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