Journal
ORGANIC LETTERS
Volume 4, Issue 3, Pages 359-362Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol017011x
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[GRAPHICS] he sodium salt of hypophosphorous acid is shown to act as a double radical precursor in a double, sequential radical addition on 3-exo-methylenefuranose derivative 14 and 4-ethylenefuranose 10 to furnish phosphinates 18d in good overall yields. Unambiguous structural assignment establishes the high diastereoselection of the process.
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