Journal
ORGANIC LETTERS
Volume 4, Issue 3, Pages 323-326Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol016793r
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[GRAPHICS] A solid-phase synthesis of substituted benzopyranoisoxazoles is described. The six-step synthesis features a novel method of generating nitrile oxides on a polymer support followed by an intramolecular 1,3-dipolar cycloaddition with a tethered alkyne for assembly of the benzopyranolsoxazole scaffold. Furthermore, the utilization of single-bead attenuated total reflectance Fourier transform infrared (ATR-IR) microspectroscopy as an essential analytical tool for reaction optimization is highlighted.
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