Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 67, Issue 4, Pages 1411-1413Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo0161678
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Funding
- NIEHS NIH HHS [ES07320, ES05931, ES05705] Funding Source: Medline
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The one-step synthesis of amino-polyether tritert-butyl ester monomer 2, by condensation of TRIS with tert-butyl acrylate, is reported. The nitrogen of the monomer can be protected with a Cbz group; subsequent removal of the tert-butyl esters with formic acid affords a triacid that is coupled to three monomers to afford an orthogonally protected two-generation, trifurcated polyether-polyamide dendron. The Cbz protecting group may be removed from the second-generation dendron without disturbing the tertbutyl esters of the periphery.
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