Journal
ORGANIC LETTERS
Volume 4, Issue 5, Pages 859-862Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0255965
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During studies directed toward the total synthesis of garsubellin A, a concise stereocontrolled synthesis of the 18-epi-tricyclic compound 3 was achieved. Key steps were a one-pot stereoselective construction of the bicyclic lactone 23 followed by a formal migration to the bicyclo-[3.3.1]nonane-1,3,5-trione and an intramolecular Wacker-type tetrahydrofuran ring formation.
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