Journal
ORGANIC LETTERS
Volume 4, Issue 5, Pages 843-846Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol025544f
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A two-step, high-yielding synthesis of Delta(2)-thiazolines containing a difluoromethylphosphonate diester moiety has been devised using a building block approach. Racemic or chiral beta-amino alcohols and diols were coupled with methyl difluoro(diethoxyphosphono)dithioacetate to give predominantly the corresponding beta-hydroxythioamides, which were then cyclized to provide a series of novel substituted Delta(2)-thiazolines.
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