Journal
JOURNAL OF ELECTROANALYTICAL CHEMISTRY
Volume 521, Issue 1-2, Pages 168-174Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/S0022-0728(02)00690-3
Keywords
rhenium; electrodeposition; voltammetry; ellipsometry; film growth
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Films obtained after cathodic polarization at E-c, -0.2 V less than or equal to E-c less than or equal to 0.1 V (vs. RHE), in aqueous acid perrhenate have been investigated using cyclic voltammetry and ellipsometry. The thickness and optical indices corresponding to the electrodeposited rhenium layer were calculated. The results indicate the formation of a composite layer, with a volumetric fraction of about 30% of metallic rhenium and hydrogen occlusion. (C) 2002 Elsevier Science B.V. All rights reserved.
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