Journal
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS
Volume 58, Issue -, Pages I45-I46Publisher
BLACKWELL MUNKSGAARD
DOI: 10.1107/S0108270102002032
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In K4Sn9, which crystallizes with a new structure type, the Sn atoms form isolated Wade nido-[Sn-9](4-) clusters of approximate C-4v symmetry (monocapped square antiprisms), with Sn-Sn distances ranging from 2.9264 (9) to 3.348 (1) Angstrom. The cluster anions are separated by K+ cations and are in a hexagonal close-packed arrangement.
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