Journal
JOURNAL OF ORGANOMETALLIC CHEMISTRY
Volume 649, Issue 1-2, Pages 50-54Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/S0022-328X(01)01452-8
Keywords
sodium; 15-crown-5; cyclopentadienyl; indenyl; fluorenyl
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The sodium complexes [NaC5H5(15-crown-5)] (1a). [NaC9H7(15-crown-5)] (1b), and [NaC13H9(15-crown-5)] (1c, C5H5 = cyclopentadienyl, C9H7 = indenyl, C13H9 = fluorenyl) were synthesized from NaC5H5, NaC9H7, NaC13H9, and 15-crown-5. Single crystal X-ray diffraction analyses were carried out for all three compounds 1a, 1b, 1c, and show that monomeric units were present in the solid state with the organic aromatic anion coordinated to the sodium cation via the five-membered ring. (C) 2002 Elsevier Science B.V. All rights reserved.
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