Journal
TETRAHEDRON
Volume 58, Issue 16, Pages 3137-3143Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4020(02)00278-8
Keywords
diazoamide; piperidin-2-one; carbene insertion; cyclopropanation; olefination; pyrazoline
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The efficient synthesis of 3-diazo-piperidin-2-one, from L-ornithine, in two steps is reported. The chemistry of this new cyclic alpha-diazoamide was explored and allows the rapid access to a wide range of 3-substituted piperidin-2-one derivatives. (C) 2002 Elsevier Science Ltd. All rights reserved.
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