Journal
ORGANIC LETTERS
Volume 4, Issue 11, Pages 1943-1946Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol025968+
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[GRAPHICS] A highly diastereoselective single-step cyclization reaction provides access to the bicyclo[3.3.1]nonane core of the polyprenylated phloroglucin natural product garsubellin A. Further elaboration to a more functionalized analogue involves a sequential Claisen rearrangement/Grubbs olefin cross-metathesis strategy. Additionally, this strategy was extended to the preparation of the bis-quaternary carbon array found at the bridgehead positions of the phloroglucin natural products.
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