Journal
ORGANIC LETTERS
Volume 4, Issue 11, Pages 1939-1942Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0259793
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[GRAPHICS] Trisubstituted alkenes have been prepared via intermolecular olefin cross-metathesis (CM) between alpha-olefins and symmetrically 1,1-disubstituted olefins using an imidazolylidene ruthenium benzylidene complex. Of particular interest is the synthesis of isoprenoid/prenyl groups by a simple solvent-free CM reaction with isobutylene. In addition, prenyl groups can also be installed by a cross-metathesis of 2-methyl-2-butene with a variety of alpha-olefins at room temperature with low catalyst loadings.
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