Journal
JOURNAL OF APPLIED POLYMER SCIENCE
Volume 133, Issue 2, Pages -Publisher
WILEY
DOI: 10.1002/app.42397
Keywords
biomaterials; cellulose and other wood products; extrusion; morphology; packaging
Categories
Funding
- Hungarian Research Fund (OTKA) [K 109409]
- National Excellence Program Elaborating and operating an inland student and researcher personal support system [TAMOP 4.2.4. A/1-11-1-2012-0001]
- European Union
- European Social Fund
- New Szechenyi Plan [TAMOP-4.2.1/B-09/1/KMR-2010-0002]
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In this study thermoplastic starch (TPS) matrix-based microfibrillated cellulose (MFC) reinforced microcomposites were prepared via extrusion compounding in one-step. Starch was plasticized with a combination of glycerol and water. The native starch/glycerol and the plasticized starch/water ratios were set for 4/1 and 6/1, respectively. Two different MFC types (of varying mean length and diameter) were incorporated up to 20 wt % in the plasticizer-containing premix prior to its compounding in a twin-screw extruder. The mechanical properties of the TPS biocomposites were markedly enhanced by the introduction of MFC. The yield strength was improved by similar to 50%, whereas the stiffness by similar to 250% upon adding 20 wt % MFC compared to the parent TPS. Dynamic mechanical analysis (DMA) revealed that the reinforcing effect of the MFC was more prominent in the starch-than in the glycerol (plasticizer)-rich phase of the TPS. The mean length and diameter of the MFCs, yielding similar aspect ratio values lying below the estimated critical one, influenced the mechanical, thermal, and thermo-mechanical properties marginally. (C) 2015 Wiley Periodicals, Inc.
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