Journal
TETRAHEDRON LETTERS
Volume 43, Issue 24, Pages 4317-4319Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(02)00800-6
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Chemoselective bis-trifluoromethylation of acyl chlorides using the CF3I/TDAE-derived nucleophilic trifluoromethyl anion reagent is reported. Very high yields are obtained of an ester product formed by sequential nucleophilic bis-trifluoromethylation, followed by acylation of the resultant alcoholate. (C) 2002 Elsevier Science Ltd. All rights reserved.
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