Journal
TETRAHEDRON LETTERS
Volume 43, Issue 27, Pages 4805-4808Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(02)00924-3
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Regioselective anodic alpha-monofluorination of oxazolidines I derived from a-amino acid was successfully carried out. This is the first example of (lie successful, direct alpha-fluorination of protected amino acids. Anodic fluorination of methyl N-acetyl pyroglutamate also provided the corresponding alpha-fluorinated product in moderate yield, while the anodic fluorination of an open-chain alpha-amino acid. N-(carboethoxy)methlphathalimide, was unsuccessful. (C) 2002 Elsevier Science Ltd. All rights reserved.
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