Journal
CHEMICAL PHYSICS LETTERS
Volume 360, Issue 5-6, Pages 501-508Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/S0009-2614(02)00827-8
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The single crystals of the 'tetragonal' C-60 Polymer were prepared by the polymerization of C-60 single crystals under a pressure of 2.5 GPa at 500 degreesC. The X-ray structural analysis resulted in the orthorhombic space group Immm; a = 9.026(2) Angstrom, b = 9.083(2) Angstrom, c = 15.077(3) Angstrom, and Z = 2; R1/wR2 = 0.0731/0.1719 for 654 observed reflections and 74 variables. The crystal structure represents a pseudo-tetragonal packing of translationally identical adjacent two-dimensional (2D) layers formed by the polymerization of C-60 molecules via [2+2] cycloaddition. (C) 2002 Published by Elsevier Science B.V.
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