Journal
JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
Volume 43, Issue 3-4, Pages 179-182Publisher
SPRINGER
DOI: 10.1023/A:1021265822247
Keywords
carbon dioxide; inclusion complex; p-t-butylcalix[4] arene; supercritical
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In this paper we report evidence for an inclusion complex between carbon dioxide and p-t-butylcalix[4] arene. The complex was studied with infrared spectroscopy, single-crystal X-ray diffraction, solid-state NMR, and thermogravimetric analysis. Results indicate that 70% of the p-t-butylcalix[ 4] arene cavities could be occupied by a CO2 molecule following exposure at 30 MPa and 40degreesC.
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