Journal
TETRAHEDRON LETTERS
Volume 43, Issue 32, Pages 5607-5609Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(02)01116-4
Keywords
microwave-accelerated reaction; DBU; nucleophilic catalyst; methylation; dimethyl carbonate; phase-transfer reagent
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An environmentally friendly process for the esterification of carboxylic acids with dimethyl carbonate can be accelerated by employing a combined strategy: using 1,8-diazabicyclo[5,4,0]undec-7-ene (DBU) as the catalyst (chemical means) and microwave as the energy Source (Physical means). This approach provides synthetic advantages, niches, and upscalability. (C) 2002 Published by Elsevier Science Ltd.
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