Journal
ORGANIC LETTERS
Volume 4, Issue 17, Pages 2993-2995Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol026401w
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Triethylborane-induced hydrometalation of alkynes proceeds in an anti manner to afford the corresponding (Z)-alkenylmetal compounds stereoselectively, where dichloroindium hydride would play a key role. A variety of functional groups including hydroxy, carbonyl, and carboxy groups were tolerant under the reaction conditions. Following iodolysis and cross-coupling reaction of the (Z)-alkenylmetal species show the usefulness of this strategy.
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