Journal
CHEMISTRY LETTERS
Volume -, Issue 9, Pages 924-925Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.2002.924
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According to the results of a model study using benzyl alcohol, pseudorotaxane with terminal hydroxy group on the axle was acylated with S-2-pyridyl 3,5-dimethylthiobenzoate in the presence of tributylphosphine to produce rotaxane in 85% yield. Optically active [2]rotaxane and [3]rotaxane were readily synthesized by this method.
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