Journal
INORGANIC CHEMISTRY COMMUNICATIONS
Volume 5, Issue 11, Pages 924-928Publisher
ELSEVIER
DOI: 10.1016/S1387-7003(02)00602-0
Keywords
mono-; di- and tri-nuclear Ni(II) complexes; urea adduct; pyridine bound mononuclear Ni(II) complex; N-; O-donor molecules
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A series of mono-, di- and tri-nuclear Ni(II) complexes of N, O-donating molecules possessing -H2C-NH- and -HC=N-moieties have been synthesized and characterized and the structures have been determined by single crystal X-ray diffraction. All these exhibited interesting molecular packing in their crystal lattices. Di-nuclear complexes were found to be cleaved in pyridine to result in mononuclear ones with additional coordinations being provided by pyridine. Di-nuclear complexes were found to form urea adducts as demonstrated based on absorption and vibrational studies. (C) 2002 Elsevier Science B.V. All rights reserved.
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