Journal
SYNTHESIS-STUTTGART
Volume -, Issue 15, Pages 2215-2219Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-2002-34839
Keywords
cyclization; halogenation; electron transfer; halide oxidation
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beta-Dicarbonyl compounds, such as dimethyl malonate derivatives and methyl acetoacetate derivatives, were electrooxidized in methanol in the presence of halogen ions to afford the corresponding dimethyl alpha-halomalonates and methyl alpha-halocarboxylates. Electrooxidation of bis(beta-dimethoxycarbonyl) derivatives similarly afforded cyclic compounds and dihalides.
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