Journal
JOURNAL OF RESEARCH OF THE NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY
Volume 107, Issue 6, Pages 703-718Publisher
NATL INST STANDARDS & TECHNOLOGY-NIST
DOI: 10.6028/jres.107.057
Keywords
Corning; epma; glass; homogeneity; microprobe; standard; trace element; eds; 95IRV; 95IRW; 95IRX
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The preparation, synthesis, and characterization of Corning trace-element glasses 95IRV, 95IRW, and 95IRX by bulk chemical and electron microprobe techniques is discussed. Working values for the doped elements in the 95-series glasses are established. Blank values have been determined by both bulk chemical and electron microprobe analysis, and important x-ray interferences are highlighted. Chemical homogeneity both within a rod cross-section, and along cane length has been documented. These glasses are standard reference materials intended for use as both primary and secondary electron microprobe standards.
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