Journal
MATERIALS LETTERS
Volume 57, Issue 9-10, Pages 1604-1611Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/S0167-577X(02)01040-6
Keywords
tin oxide; citric acid; nanocrystalline; citrate glass; powder XRD; TEM
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Nanocrystalline SnO2 has been synthesized by liquid mix technique using citric acid as the complexing agent. The tin oxide powder obtained at different calcination temperatures (773 - 1223 K) is characterized using powder X-ray diffraction (XRD), SEM, TEM, TG-DTG and UV spectroscopic techniques. The material obtained is nanocrystalline, having particle size in the range of 10 - 14 nm. The technique is cost-effective and yields the desired product at temperatures as low as 773 K. (C) 2002 Elsevier Science B.V. All rights reserved.
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