4.3 Article

Highly α-stereoselective one-pot sequential glycosylation using glucosyl thioformimidate derivatives

Journal

CHEMISTRY LETTERS
Volume 32, Issue 2, Pages 172-173

Publisher

CHEMICAL SOC JAPAN
DOI: 10.1246/cl.2003.172

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Several trisaccharides were prepared by efficient highly astereoselective one-pot sequential glycosylation using glucosyl p-trifluoromethylbenzylthio-p-trifluoromethylphenyl formimidates (abbreviated to: glucosyl thioformimidates) in the presence of a catalytic amount of TfOH. Factors that controlled the high astereoselectivity were determined by characteristic properties of thioformimidate groups contained both in glucosyl donor and acceptor.

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