Journal
ORGANIC LETTERS
Volume 5, Issue 3, Pages 337-339Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0273553
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A new route, of potential strategic importance, to a difluorosugar analogue has been developed. Key steps included a Stille coupling and a highly regio- and enantioselective dihydroxylation of a highly substituted diene. Protecting groups were chosen to enhance the reactivity of the disubstituted allylic fragment in the AD reaction and allow deprotection under orthogonal conditions.
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