Journal
CARBOHYDRATE RESEARCH
Volume 338, Issue 5, Pages 447-449Publisher
ELSEVIER SCI LTD
DOI: 10.1016/S0008-6215(02)00481-0
Keywords
zinc triflate; benzoyl bromide; glycosyl bromide; protecting groups
Funding
- NHLBI NIH HHS [HL62244] Funding Source: Medline
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A simple and efficient method is developed for the chemoselective one-pot conversion of ethers (benzyl, TBDMS and acetal) to the corresponding benzoates by zinc triflate-catalyzed deprotection and benzoylation by benzoyl bromide. In the same reaction, methyl or p-methoxyphenyl glycosides are converted into glycosyl bromides that are useful in glycosylation reactions. (C) 2003 Elsevier Science Ltd. All rights reserved.
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