Journal
JOURNAL OF ELECTRON SPECTROSCOPY AND RELATED PHENOMENA
Volume 129, Issue 1, Pages 1-8Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/S0368-2048(03)00016-1
Keywords
NEXAFS; calibration; normalization; carbon edge
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Using high-brilliance synchrotron radiation and an ultrahigh-resolution monochromator a wealth of new fine structures can be observed in near-edge X-ray absorption spectra. The potential information gain, however, requires an accurate calibration of the energy scale and a perfect intensity normalization in order to avoid erroneous results, e.g., the occurrence of spurious peaks. By means of the most problematic C 1s edge it is shown how large these effects can be and how appropriate energy calibration and intensity normalization can be achieved. (C) 2003 Elsevier Science B.V. All rights reserved.
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