Journal
TETRAHEDRON
Volume 59, Issue 14, Pages 2555-2560Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4020(03)00250-3
Keywords
polyfluoroalkyl iodide; gamma-butyrolactones; sodium dithionite; polyfluoroalkyl-lactonization; 4-pentenoic acid
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The polyfluoroalkyl-lactonization of 4-pentenoic acids having a substituent at the 2 or 3 position with the polyfluoroalkyl iodides initiated by sodium dithionite was realized in good yields. A new and efficient method for the synthesis of fluorine-containing gamma-lactones is described. (C) 2003 Elsevier Science Ltd. All rights reserved.
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