Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 68, Issue 10, Pages 4079-4082Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo020559c
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An efficient improved procedure for the synthesis of beta-acetamido carbonyl compounds is developed by a cobalt(II) chloride-catalyzed three-component coupling protocol. The procedure is also amenable to the synthesis of gamma-lactams by a three-component coupling reaction with use of 2-carbomethoxybenzaldehyde. The beta-acetamido carbonyl compounds derived from 2-carbomethoxybenzaldehyde are useful intermediates as they can be transformed to the corresponding gamma-lactams on treatment with base.
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