Journal
CHEMISTRY OF MATERIALS
Volume 15, Issue 10, Pages 2017-2024Publisher
AMER CHEMICAL SOC
DOI: 10.1021/cm0213218
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Using a two-step procedure based on (i) anchoring an organogold precursor within the channels of functionalized ordered mesoporous silica containing mercapto groups; (ii) followed by chemical reduction, we prepared materials containing gold (0) nanoparticles exclusively located within the pore channels. By modifying the organogold precursor/mercapto groups ratio, we demonstrate the necessity of the complexation of the organogold precursor prior to reduction. Using this methodology, gold content as high as 16.1 wt % with a narrow size distribution of nanoparticles regularly distributed within the pores of the material was achieved.
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