Journal
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE
Volume 629, Issue 7-8, Pages 1147-1152Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/zaac.200300010
Keywords
molecular quadrangles; cyanides; iron; nickel; zinc
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Using cis-(bpy)(2)FeX2 building blocks the stepwise formation of molecular quadrangles with Fe2M2(mu-CN)(4) frameworks was achieved. Intermediates were dinuclear complexes with Fe-CN-M units (M = Ni, Cu) and trinuclear complexes with Zn(NC-Fe)(2) and Fe(CN-M)(2) units (M = Ni, Cu). Spectroscopic and electrochemical data were obtained. The structures of the trinuclear Fe(CN-CU)(2) complex and the tetranuclear Fe-4(mu-CN)(4) complex were determined.
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