Journal
COMPTES RENDUS CHIMIE
Volume 6, Issue 7, Pages 657-662Publisher
ELSEVIER FRANCE-EDITIONS SCIENTIFIQUES MEDICALES ELSEVIER
DOI: 10.1016/S1631-0748(03)00118-8
Keywords
functionalized bis(ethylenedithio)tetrathiafulvalene; crystal structure; electrochemistry
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Novel functionalized bis(ethylenedithio)tetrathiafulvalene (BEDT-TTF) derivatives 4 and 5 have been synthesized in good yields from cyano precursor via a cross-coupling reaction. Their redox potentials have been studied by cyclic voltammetry in a dichloromethane solution: this indicated that they are slightly weaker electron donors than BEDT-TTF. Compound 4 has been studied by X-ray crystallography; this revealed that, in the crystal, the molecules were held together by some unconventional C-(HN)-N-... and C-(HS)-S-... hydrogen bonds. (C) 2003 Published by Editions scientifiques et medicales Elsevier SAS on behalf of Academie des sciences.
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