Journal
JOURNAL OF SEPARATION SCIENCE
Volume 26, Issue 11, Pages 1057-1062Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/jssc.200301447
Keywords
gaseous standard mixtures; surface compounds; glass fiber; chemical modification; thermal decomposition; calibration; ethene
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The use of glass fiber as a support material for a surface compound serving to generate gaseous standard mixtures of ethene is described. The technique is based on the process of thermal decomposition of the surface compound in a desorber connected on-line via a multi-port valve to the calibrated device. The surface compound undergoes thermal decomposition at 245degreesC, yielding known amounts of ethene. The method enables on-line preparation of a standard mixture immediately before the calibration step. Consequently, it can be also applied for the generation of standard mixtures containing volatile, malodorous, unstable, and toxic compounds.
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