Journal
TETRAHEDRON LETTERS
Volume 44, Issue 29, Pages 5495-5498Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(03)01328-5
Keywords
nitromethane; C-glycoside; DBU
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Mechanistic intermediates, and thermodynamically favored side products, in the Henry condensations of partially protected and non-protected pyranoses with a free anomeric hemiacetal function with nitromethane in various solvents for the kinetically controlled syntheses of C-glycopyranosides in the presence of DBU/molecular sieve catalyst system were identified. (C) 2003 Elsevier Science Ltd. All rights reserved.
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