Journal
CHEMICAL ENGINEERING RESEARCH & DESIGN
Volume 81, Issue A7, Pages 760-765Publisher
INST CHEMICAL ENGINEERS
DOI: 10.1205/026387603322302931
Keywords
nitration; toluene; ureas; online analysis; mechanistic studies; monitoring of microreactor performance
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Online analytical techniques were used to monitor fast and strong exothermic nitrations in microreactors. Mechanistic studies were conducted by using online FTIR microscopy to identify key intermediates in microchannels. IR spectroscopy, thermography and HPLC were used to investigate the influence of changing process conditions, to control the completeness of conversion and to monitor the stability of the entire microreaction process.
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